TY - JOUR
T1 - Small-angle X-ray scattering station 4C2 BL of Pohang accelerator laboratory for advance in Korean polymer science
AU - Yoon, Jinhwan
AU - Kim, Kwang Woo
AU - Kim, Jehan
AU - Heo, Kyuyoung
AU - Jin, Kyeong Sik
AU - Jin, Sangwoo
AU - Shin, Tae Joo
AU - Lee, Byeongdu
AU - Rho, Yecheol
AU - Ahn, Byungcheol
AU - Ree, Moonhor
PY - 2008/10
Y1 - 2008/10
N2 - There are two beamlines (BLs), 4C1 and 4C2, at the Pohang Accelerator Laboratory that are dedicated to small angle X-ray scattering (SAXS). The 4C1 BL was constructed in early 2000 and is open to public users, including both domestic and foreign researchers. In 2003, construction of the second SAXS BL, 4C2, was complete and commissioning and user support were started. The 4C2 BL uses the same bending magnet as its light source as the 4C1 BL. The 4C1 BL uses a synthetic double multilayer monochromator, whereas the 4C2 BL uses a Si(111) double crystal monochromator for both small angle and wide angle X-ray scattering. In the 4C2 BL, the collimating mirror is positioned behind the monochromator in order to enhance the beam flux and energy resolution. A toroidal focusing mirror is positioned in front of the monochromator to increase the beam flux and eliminate higher harmonics. The 4C2 BL also contains a digital cooled charge coupled detector, which has a wide dynamic range and good sensitivity to weak scattering, thereby making it suitable for a range of SAXS and wide angle X-ray scattering experiments. The general performance of the 4C2 BL was initially tested using standard samples and further confirmed by the experience of users during three years of operation. In addition, several grazing incidence X-ray scattering measurements were carried out at the 4C2 BL.
AB - There are two beamlines (BLs), 4C1 and 4C2, at the Pohang Accelerator Laboratory that are dedicated to small angle X-ray scattering (SAXS). The 4C1 BL was constructed in early 2000 and is open to public users, including both domestic and foreign researchers. In 2003, construction of the second SAXS BL, 4C2, was complete and commissioning and user support were started. The 4C2 BL uses the same bending magnet as its light source as the 4C1 BL. The 4C1 BL uses a synthetic double multilayer monochromator, whereas the 4C2 BL uses a Si(111) double crystal monochromator for both small angle and wide angle X-ray scattering. In the 4C2 BL, the collimating mirror is positioned behind the monochromator in order to enhance the beam flux and energy resolution. A toroidal focusing mirror is positioned in front of the monochromator to increase the beam flux and eliminate higher harmonics. The 4C2 BL also contains a digital cooled charge coupled detector, which has a wide dynamic range and good sensitivity to weak scattering, thereby making it suitable for a range of SAXS and wide angle X-ray scattering experiments. The general performance of the 4C2 BL was initially tested using standard samples and further confirmed by the experience of users during three years of operation. In addition, several grazing incidence X-ray scattering measurements were carried out at the 4C2 BL.
KW - Beamline
KW - Detector
KW - Grazing-incidence X-ray scattering
KW - In-situ X-ray scattering
KW - Pohang accelerator laboratory
KW - Polymers
KW - Small-angle X-ray scattering
KW - Synchrotron radiation sources
KW - Transmission X-ray scattering
KW - Wide-angle X-ray scattering
UR - http://www.scopus.com/inward/record.url?scp=56049092981&partnerID=8YFLogxK
U2 - 10.1007/BF03218563
DO - 10.1007/BF03218563
M3 - Review article
AN - SCOPUS:56049092981
SN - 1598-5032
VL - 16
SP - 575
EP - 585
JO - Macromolecular Research
JF - Macromolecular Research
IS - 7
ER -